Formation of Isoamyl Acetate Lab Report Example | Topics and Well Written Essays - 250 words

Formation of Isoamyl Acetate - Lab tell ExampleDuring reflux a colour change from colourless to slight yellow was observed. After 15 minute reflux the mixture was everyowed to cool and 1M sodium hydroxide solution was used for the neutralisation. Strong banana smell was detected. To the obtained solution a portion of diethyl ether was added. As two layers formed, sparatory funnel was used to transpose the diethyl ether layer. Extraction was conducted several times after which all the produced diethyl ether layers were combined, dried and heated until all diethyl layer evaporated. The described manipulations afforded 1.52 g. of isoamyl ester (25.42%).It is expected that the boiling point of isoamyl acetate pull up stakes be 1420C, however this temperature will be lower of traces of diethyl ether remained. Regarding IR results, it is expected that there will be no signals in the region 3000-4000 cm-1. If there are then traces of acetic acid or alcohol remained in the product. Also , symptomatic signals in the region 1500-2000 cm-1 should point out to the presence of C=O group. The fingerprint region should be compared with the isoamyl acetate spectrum from the database (Clayden, et al.,